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Laser sintering of Cu nanoparticles on PET polymer substrate for printed electronics at different wavelengths

Juan Carlos HERNANDEZ-CASTANEDA, Boon Keng LOK, Hongyu ZHENG

《机械工程前沿（英文）》 2020年第15卷第2期页码 303-318 doi: 10.1007/s11465-019-0562-x

摘要： This study explores the feasibility of different laser systems to sinter screen-printed lines from nonconductive copper nanoparticles (Cu NPs) on polyethylene terephthalate polymer film. These materials are commonly used in manufacturing functional printed electronics for large-area applications. Here, optical and thermal characterization of the materials is conducted to identify suitable laser sources and process conditions. Direct diode (808 nm), Nd:YAG (1064 nm and second harmonic of 532 nm), and ytterbium fiber (1070 nm) lasers are explored. Optimal parameters for sintering the Cu NPs are identified for each laser system, which targets low resistivity and high processing speed. Finally, the quality of the sintered tracks is quantified, and the laser sintering mechanisms observed under different wavelengths are analyzed. Practical considerations are discussed to improve the laser sintering process of Cu NPs.

关键词： laser sintering copper nanoparticles printed electronics

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Development of lunar regolith composite and structure via laser-assisted sintering

《机械工程前沿（英文）》 doi: 10.1007/s11465-021-0662-2

摘要： Aiming at the exploration and resource utilization activities on the Moon, in situ resource utilization and in situ manufacturing are proposed to minimize the dependence on the ground transportation supplies. In this paper, a laser-assisted additive manufacturing process is developed to fabricate lunar regolith composites with PA12/SiO₂ mixing powders. The process parameters and composite material compositions are optimized in an appropriate range through orthogonal experiments to establish the relationship of process–structure–property for lunar regolith composites. The optimal combination of composite material compositions and process parameters are mixing ratio of 50/50 in volume, laser power of 30 W, scanning speed of 3500 mm/s, and scanning hatch space of 0.2 mm. The maximum tensile strength of lunar regolith composites reaches 9.248 MPa, and the maximum depth of surface variation is 120.79 μm, which indicates poor powder fusion and sintering quality. Thereafter, the mechanical properties of laser-sintered lunar regolith composites are implemented to the topology optimization design of complex structures. The effectiveness and the feasibility of this laser-assisted process are potentially developed for future lightweight design and manufacturing of the solar panel installed on the lunar rover.

关键词： in situ manufacturing laser-assisted powder fusion process mechanical properties topological structure design

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Two-dimensional modeling of sintering of a powder layer on top of nonporous substrate

Tiebing CHEN, Yuwen ZHANG,

《机械工程前沿（英文）》 2010年第5卷第2期页码 143-148 doi: 10.1007/s11465-010-0006-0

摘要： Selective laser sintering (SLS) of a two-component metal powder layer on the top of multiple sintered layers by a moving Gaussian laser beam is modeled. The loose metal powder layer is composed of a powder mixture with significantly different melting points. The physical model that accounts the shrinkage induced by melting is described by using a temperature-transforming model. The effects of the porosity and the thickness of the atop loose powder layer with different numbers of the existing sintered metal powder layers below on the sintering process are numerically investigated. The present work will provide a better understanding to simulate much more complicated three-dimensional SLS process.

关键词： laser sintering melting solidification heat transfer

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Stabilization of hexavalent chromium with pretreatment and high temperature sintering in highly contaminated

Haiyan Mou, Wenchao Liu, Lili Zhao, Wenqing Chen, Tianqi Ao

《环境科学与工程前沿（英文）》 2021年第15卷第4期 doi: 10.1007/s11783-020-1353-7

摘要： Abstract • Separate reduction and sintering cannot be effective for Cr stabilization. • Combined treatment of reduction and sintering is effective for Cr stabilization. • Almost all the Cr in the reduced soil is residual form after sintering at 1000°C. This study explored the effectiveness and mechanisms of high temperature sintering following pre-reduction with ferric sulfate (FeSO4), sodium sulfide (Na2S), or citric acid (C6H8O7) in stabilizing hexavalent chromium (Cr(VI)) in highly contaminated soil. The soil samples had an initial total Cr leaching of 1768.83 mg/L, and Cr(VI) leaching of 1745.13 mg/L. When FeSO4 or C6H8O7 reduction was followed by sintering at 1000°C, the Cr leaching was reduced enough to meet the Safety Landfill Standards regarding general industrial solid waste. This combined treatment greatly improved the stabilization efficiency of chromium because the reduction of Cr(VI) into Cr(III) decreased the mobility of chromium and made it more easily encapsulated in minerals during sintering. SEM, XRD, TG-DSC, and speciation analysis indicated that when the sintering temperature reached 1000°C, almost all the chromium in soils that had the pre-reduction treatment was transformed into the residual form. At 1000°C, the soil melted and promoted the mineralization of Cr and the formation of new Cr-containing compounds, which significantly decreased subsequent leaching of chromium from the soil. However, without reduction treatment, chromium continued to leach from the soil even after being sintered at 1000°C, possibly because the soil did not fully fuse and because Cr(VI) does not bind with soil as easily as Cr(III).

关键词： Chromium Heavy contaminated soil Reduction Sintering Stabilization Speciation

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Fabrication of form stable NaCl-Al2O3 composite for thermal energy storage by cold sintering process

Bilyaminu Suleiman, Qinghua Yu, Yulong Ding, Yongliang Li

《化学科学与工程前沿（英文）》 2019年第13卷第4期页码 727-735 doi: 10.1007/s11705-019-1823-2

摘要： A form stable NaCl-Al O (50-50 wt-%) composite material for high temperature thermal energy storage was fabricated by cold sintering process, a process recently applied to the densification of ceramics at low temperature ˂ 300°C under uniaxial pressure in the presence of small amount of transient liquid. The fabricated composite achieved as high as 98.65% of the theoretical density. The NaCl-Al O composite also retained the chloride salt without leakage after 30 heating-cooling cycles between 750°C–850°C together with a holding period of 24 h at 850°C. X-ray diffraction measurements indicated congruent solubility of the alumina in chloride salt, excellent compatibility of NaCl with Al O , and chemical stability at high temperature. Structural analysis by scanning electron microscope also showed limited grain growth, high density, uniform NaCl distribution and clear faceted composite structure without inter-diffusion. The latent heat storage density of 252.5 J/g was obtained from simultaneous thermal analysis. Fracture strength test showed high sintered strength around 5 GPa after 50 min. The composite was found to have fair mass losses due to volatilization. Overall, cold sintering process has the potential to be an efficient, safe and cost-effective strategy for the fabrication of high temperature thermal energy storage materials.

关键词： cold sintering process composite fabrication thermal energy storage phase change materials

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Current understanding and applications of the cold sintering process

Tong Yu, Jiang Cheng, Lu Li, Benshuang Sun, Xujin Bao, Hongtao Zhang

《化学科学与工程前沿（英文）》 2019年第13卷第4期页码 654-664 doi: 10.1007/s11705-019-1832-1

摘要： In traditional ceramic processing techniques, high sintering temperature is necessary to achieve fully dense microstructures. But it can cause various problems including warpage, overfiring, element evaporation, and polymorphic transformation. To overcome these drawbacks, a novel processing technique called “cold sintering process (CSP)” has been explored by Randall et al. CSP enables densification of ceramics at ultra-low temperature (≤300°C) with the assistance of transient aqueous solution and applied pressure. In CSP, the processing conditions including aqueous solution, pressure, temperature, and sintering duration play critical roles in the densification and properties of ceramics, which will be reviewed. The review will also include the applications of CSP in solid-state rechargeable batteries. Finally, the perspectives about CSP is proposed.

关键词： cold sintering process processing variables solid-state rechargeable batteries

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激光去除与连接技术发展研究

陈俐,巩水利,何恩光

《中国工程科学》 2020年第22卷第3期页码 78-84 doi: 10.15302/J-SSCAE-2020.03.012

摘要：

随着激光技术的发展，激光去除与连接技术深刻影响着制造业技术的发展，并以柔性、高效、高质的综合优势成为不可或缺的先进制造技术。在先进制造智能化发展的时代，激光技术、数字信息技术等的融合必将推动激光去除与连接技术的应用发展与创新。本文选取工业应用最广的激光焊接、激光切割、激光打孔、激光打标4 种激光去除与连接技术，概述了激光去除与连接技术的应用现状，分析了其在支撑先进制造发展过程中存在的问题。研究表明，激光去除与连接技术的发展应注重工艺基础和装备研究一体化的研究，解决激光加工单元部件、激光加工工艺、智能集成各环节的关键技术，强化工艺基础研究平台建设，关注技术创新和人才培养的多维度结合，以促进激光去除与连接技术从工艺应用开发到装备市场保障的生态链式的协同发展。

关键词：激光加工激光焊接激光切割激光打孔激光打标

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Temperature field simulation of laser homogenizing equipment

Juanjuan WANG, Yunshan WANG, Fudong ZHU

《机械工程前沿（英文）》 2009年第4卷第1期页码 49-52 doi: 10.1007/s11465-009-0005-1

摘要： The laser homogenizing equipment was devised using the ring scanning principle. Its working principle is explained. A laser scanning ring facula is obtained when the laser beam goes through the equipment’s optical system rotating with high-frequency. The scanning ring facula’s mathematic model is established based on the temperature field’s superposing principle. The ring facula’s light intensity distribution and temperature distribution characteristics are achieved by simulating its temperature field. By studying the effect of parameters on the temperature field, the best parameter can be found. Results show that favorable temperature distribution characteristics can be attained by choosing appropriate parameters, and even the thermal effect can be realized by utilizing the circumference power compensating for the heat exchange lost in the horizontal direction. The uniform hardness layer and better process quality can be attained using the ring facula optimized for metal laser heat treatment.

关键词： laser homogenizing technology laser scanning ring facula temperature field

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我国激光技术与应用2035 发展战略研究

“我国激光技术与应用2035 发展战略研究”项目综合组

《中国工程科学》 2020年第22卷第3期页码 1-6 doi: 10.15302/J-SSCAE-2020.03.001

摘要：

为促进激光技术及应用的发展，中国工程院于2018 年启动了“我国激光技术与应用2035 发展战略研究”重点咨询项目，本文是项目研究综合报告，文章简要分析了激光技术及在科研与产业中的工具性、引领性和颠覆性作用，分析了我国激光技术在前沿激光、制造加工、信息通信、医疗诊治等领域的科研和应用的发展现状，梳理了多个制约加速发展的问题，提出了我国激光技术及应用2035 年发展目标设想：强化顶层统筹谋划，引领我国激光技术与应用产业快速发展；加强基础研究，聚力突破产业化发展中的重大基础问题、共性技术基础和基础材料、器件；设立应用研发专项，打造多个新激光产业链；创新产业协同机制，完善激光产业创新生态；强化激光基础教育，加大对激光及光学学科人才培养力度等政策措施建议。

关键词：激光技术激光制造激光通信激光诊疗

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Processing parameter optimization of fiber laser beam welding using an ensemble of metamodels and MOABC

《机械工程前沿（英文）》 2022年第17卷第4期 doi: 10.1007/s11465-022-0703-5

摘要： In fiber laser beam welding (LBW), the selection of optimal processing parameters is challenging and plays a key role in improving the bead geometry and welding quality. This study proposes a multi-objective optimization framework by combining an ensemble of metamodels (EMs) with the multi-objective artificial bee colony algorithm (MOABC) to identify the optimal welding parameters. An inverse proportional weighting method that considers the leave-one-out prediction error is presented to construct EM, which incorporates the competitive strengths of three metamodels. EM constructs the correlation between processing parameters (laser power, welding speed, and distance defocus) and bead geometries (bead width, depth of penetration, neck width, and neck depth) with average errors of 10.95%, 7.04%, 7.63%, and 8.62%, respectively. On the basis of EM, MOABC is employed to approximate the Pareto front, and verification experiments show that the relative errors are less than 14.67%. Furthermore, the main effect and the interaction effect of processing parameters on bead geometries are studied. Results demonstrate that the proposed EM-MOABC is effective in guiding actual fiber LBW applications.

关键词： laser beam welding parameter optimization metamodel multi-objective

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激光表面改性技术发展研究

张群莉,王梁,梅雪松,姚建华

《中国工程科学》 2020年第22卷第3期页码 71-77 doi: 10.15302/J-SSCAE-2020.03.010

摘要：

激光表面改性技术利用高能量密度的激光束对零部件局部易损易耗区域进行快速处理，获得材料表面所需性能，进而大幅延长零部件使用寿命，已在航空航天、石油化工、能源、交通、冶金等领域获得应用。本文针对激光冲击强化、激光淬火、激光熔覆3 种典型的激光表面改性技术，梳理了相应技术特点及国内外应用现状，凝练我国相关技术领域面临的差距与问题，总结激光表面改性技术的重点发展方向：专用合金材料制备、多能场激光复合表面改性、面向现场的激光再制造、激光冲击强化控形控性、激光表面改性智能化、激光表面微结构化。从政府引导、国产化创新、产业链完善、质量评价标准体系、人才培养等方面提出发展建议，以期为我国激光表面改性技术发展提供参考借鉴。

关键词：激光表面改性冲击强化淬火熔覆发展趋势

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Advances in polishing of internal structures on parts made by laser-based powder bed fusion

《机械工程前沿（英文）》 2023年第18卷第1期 doi: 10.1007/s11465-022-0724-0

摘要： The internal structures of metallic products are important in realizing functional applications. Considering the manufacturing of inner structures, laser-based powder bed fusion (L-PBF) is an attractive approach because its layering principle enables the fabrication of parts with customized interior structures. However, the inferior surface quality of L-PBF components hinders its productization progress seriously. In this article, process, basic forms, and applications relevant to L-PBF internal structures are reviewed comprehensively. The causes of poor surface quality and differences in the microstructure and property of the surface features of L-PBF inner structures are presented to provide a perspective of their surface characteristics. Various polishing technologies for L-PBF components with inner structures are presented, whereas their strengths and weaknesses are summarized along with a discussion on the challenges and prospects for improving the interior surface quality of L-PBF parts.

关键词： laser-based powder bed fusion polishing internal structures surface quality surface features post process additive manufacturing

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zone-layered trimming method for ceramic core of aero-engine blade based on an advanced reconfigurable laser

《机械工程前沿（英文）》 2022年第17卷第2期 doi: 10.1007/s11465-022-0675-5

摘要： Ceramic structural parts are one of the most widely utilized structural parts in the industry. However, they usually contain defects following the pressing process, such as burrs. Therefore, additional trimming is usually required, despite the deformation challenges and difficulty in positioning. This paper proposes an ultrafast laser processing system for trimming complex ceramic structural parts. Opto-electromechanical cooperative control software is developed to control the laser processing system. The trimming problem of the ceramic cores used in aero engines is studied. The regional registration method is introduced based on the iterative closest point algorithm to register the path extracted from the computer-aided design model with the deformed ceramic core. A zonal and layering processing method for three-dimensional contours on complex surfaces is proposed to generate the working data of high-speed scanning galvanometer and the computer numerical control machine tool, respectively. The results show that the laser system and the method proposed in this paper are suitable for trimming complex non-datum parts such as ceramic cores. Compared with the results of manual trimming, the method proposed in this paper has higher accuracy, efficiency, and yield. The method mentioned above has been used in practical application with satisfactory results.

关键词： ceramic parts trimming computer-aided laser manufacturing 3D vision reconfigurable laser processing system

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Hybrid forming mechanism of patternless casting and laser cladding

Zhongde SHAN, Fuzhen SUN, Yang LIU

《机械工程前沿（英文）》 2019年第14卷第4期页码 393-401 doi: 10.1007/s11465-019-0550-1

摘要： In accordance with the requirement of manufacturing dies quickly and economically, a hybrid forming method of stamping dies for automobile panels is proposed. The method combines digital patternless casting and high-power laser cladding. An experimental study is conducted on the hybrid forming process and its trial production and application in the manufacturing of stamping dies for typical panels. Results prove that the laser cladding layer exceeds HRC60 (Rockwell hardness) and thus meets the production efficiency requirement of automobile dies. The rate of defects is well controlled. Compared with traditional technology, this technology has remarkable advantages and advancement.

关键词： patternless casting laser cladding hybrid forming rapid tooling

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我国激光技术医疗应用和产业发展战略研究

邱海霞,李步洪,马辉,魏勋斌,杨思华,李阳,谭一舟,陈德福,赵洪友,曾晶,顾瑛

《中国工程科学》 2020年第22卷第3期页码 14-20 doi: 10.15302/J-SSCAE-2020.03.003

摘要：

激光诊疗技术在生命健康领域得到了越来越多的成功应用，成为现代医学精准诊疗的重要组成部分。本文针对激光技术医疗应用主题，重点从实际应用和产业链的视角出发，梳理我国激光技术在临床治疗、诊断和产业化方面的发展现状、前景趋势和存在问题。研究发现，尽管我国在激光治疗技术、医用激光诊疗设备及其产业发展方面均取得了长足进步，但整体而言，激光医疗技术的临床应用仍处于跟踪起步和同步发展阶段，原创性应用研究有所缺乏，医用激光设备的研发和产业化处于中低端，用于精准诊疗的超快激光器等关键技术和高端设备仍未打破国外垄断。研究建议，设立我国激光医学二级学科，加强国家级激光医疗科技创新平台建设，针对性开展激光医疗器械法规建设，出台相关政策扶持激光医疗器械产业发展，组织攻关医用激光诊疗设备关键核心技术。

关键词：激光技术医疗激光诊断激光治疗激光产业